To calculate the percent yield, we first need to determine the theoretical yield, which is the maximum amount of product that can be formed from the given amount of reactants.The balanced chemical equation for the synthesis of aspirin is:C7H6O3 salicylic acid + C4H6O3 acetic anhydride C9H8O4 aspirin + C2H4O2 acetic acid From the balanced equation, we can see that 1 mole of salicylic acid reacts with 1 mole of acetic anhydride to produce 1 mole of aspirin.First, we need to calculate the moles of salicylic acid used in the experiment:Moles of salicylic acid = mass / molar massThe molar mass of salicylic acid C7H6O3 = 7 12.01 + 6 1.01 + 3 16.00 = 138.12 g/molMoles of salicylic acid = 5 g / 138.12 g/mol = 0.0362 molNow, we can calculate the theoretical yield of aspirin:Moles of aspirin = moles of salicylic acid since they react in a 1:1 ratio = 0.0362 molThe molar mass of aspirin C9H8O4 = 9 12.01 + 8 1.01 + 4 16.00 = 180.16 g/molTheoretical yield of aspirin = moles of aspirin molar mass of aspirin = 0.0362 mol 180.16 g/mol = 6.52 gNow we can calculate the percent yield:Percent yield = actual yield / theoretical yield 100Percent yield = 4.2 g / 6.52 g 100 = 64.4%The percent yield of this experiment is 64.4%.